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Autocal Solutions Pvt. Ltd
Senior Analyst - IcpmsAutocal Solutions Pvt. Ltd • Kalyān, Thane, IN
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Senior Analyst - Icpms

Senior Analyst - Icpms

Autocal Solutions Pvt. Ltd • Kalyān, Thane, IN
8 days ago
Job description
Job Title: Senior Analyst – ICP-MS/MS Department: Water Testing & Environmental Analysis Location: Mumbai, India Reporting To: Technical Manager / Director of Testing Employment Type: Full-Time About the Role We are seeking an experienced and detail-oriented Senior Analyst – ICP-MS/MS to strengthen our Water Testing and Environmental Analysis division. The incumbent will lead elemental and heavy metal analysis across a wide range of water and environmental matrices, ensuring compliance with national and international regulatory standards. This is a technically demanding role suited to a professional with deep expertise in trace metal analysis, environmental sampling protocols, and accredited laboratory operations under ISO 17025:2017 / NABL frameworks. Key Responsibilities Instrumentation & Analysis - Operate and maintain ICP-MS/MS instruments for the quantification of trace and ultra-trace level metals and metalloids in drinking water, wastewater, surface water, groundwater, soil leachates, effluents, and sediment digests - Analyse regulated parameters including but not limited to: As, Pb, Cd, Cr, Hg, Ni, Se, Sb, Ba, Be, Tl, U, and speciated forms (e.G., Cr(VI), As(III)/As(V)) as applicable - Apply appropriate MS/MS reaction cell modes (O₂, NH₃, He) to manage polyatomic interferences common in complex environmental matrices - Execute sample digestion (microwave-assisted acid digestion per EPA 3051A/3052, aqua regia) and ensure contamination-free preparation in a clean-room or trace-metal-clean environment - Perform method calibration, internal standard correction (Sc, Ge, In, Bi, Rh), and matrix-matched calibration for high-TDS environmental samples Method Development & Validation - Develop and validate analytical methods for water and environmental samples in accordance with IS 3025, APHA (Standard Methods), EPA 200.8, ISO 17294-2, and FSSAI / MoEFCC frameworks - Conduct full method validation including LOD, LOQ, linearity, accuracy (spike recovery), precision, matrix effects, and ruggedness - Troubleshoot matrix-specific interference issues (e.G., chloride-rich coastal effluents, high-iron groundwater, industrial discharge matrices) Quality, Compliance & Documentation - Maintain all records in line with ISO 17025:2017 and NABL accreditation requirements - Prepare and review test reports, certificates of analysis (CoA), and raw data packages for regulatory submissions - Support preparation and response to NABL and MoEFCC/CPCB-related audits, including CAPA documentation - Participate in proficiency testing (PT) schemes and inter-laboratory comparison programs relevant to water and environmental testing (e.G., NABL-recognised PT providers) - Draft, review, and revise SOPs and work instructions in alignment with quality management system requirements Team & Coordination - Guide and train junior analysts on ICP-MS/MS operation, safe handling of corrosive acids, and environmental sample handling protocols - Coordinate with the sampling team on field sample collection, preservation, and chain-of-custody compliance - Liaise with the Quality Team and client-facing teams on TAT, reporting queries, and regulatory interpretation - Support business development with technical capability inputs for tenders, government agency empanelments, and client audits Qualifications & Experience - M.Sc. in Analytical Chemistry, Environmental Chemistry, or Applied Chemistry (Ph.D. or M.Tech preferred) - 4–6 years of hands-on ICP-MS or ICP-MS/MS experience in an environmental, water testing, or government-accredited laboratory - Demonstrated experience with environmental regulatory frameworks: BIS 10500, IS 3025, CPCB effluent standards, EPA 200.8, APHA Standard Methods - Working knowledge of sample preservation protocols, field blank practices, and contamination control in environmental sampling - Familiarity with NABL-accredited laboratory documentation and audit readiness Preferred Skills - Experience with speciation analysis (Cr, As, Se) using IC-ICP-MS or reaction cell-based discrimination - Exposure to ICP-OES as a complementary technique for major ions and higher-concentration matrices - Knowledge of soil/sediment digestion and total recoverable metals analysis per EPA/ISO protocols - Proficiency in instrument software (MassHunter, Syngistix, or equivalent) and LIMS-based data entry and reporting - Understanding of MoEFCC, CPCB, and state pollution control board (SPCB) regulatory reporting requirements Key Competencies - Rigorous approach to data integrity, contamination control, and trace-level cleanliness - Strong regulatory awareness across BIS, EPA, ISO, and CPCB frameworks - Ability to manage multiple sample batches and meet regulatory TAT commitments - Clear technical report writing for government, industrial, and institutional clients - Collaborative team player with mentoring capability for junior staff What We Offer - Work within a NABL/ISO 17025:2017 accredited multi-division laboratory with a dedicated Water Testing and Environmental division - Exposure to a diverse client base spanning municipal utilities, industrial effluent generators, infrastructure projects, and government regulatory bodies - Involvement in empanelment projects with CPCB, MoEFCC, and state pollution control boards - Competitive compensation with growth into technical leadership roles
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Senior Analyst - Icpms • Kalyān, Thane, IN

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